Iranian Research Organization for Science and Technology Journal of Particle Science and Technology 2423-4087 1 2 2015 05 01 A new precursor for preparation of magnetite (Fe3O4) nanoparticles 65 72 80 10.22104/jpst.2015.80 EN Mohammad Kaikhosravi Isfahan University of Technology Hassan Hadadzadeh Isfahan University of Technology Mohammad-Taghi Behnamfar Isfahan University of Technology Journal Article 2014 12 03 An anionic Fe(II) complex, (BMIM)4[Fe(CN)6] (where BMIM is 1-butyl-3-methylimidazolium), was synthesized in ionic liquid [BMIM][PF6] under reflux condition. The complex was characterized by elemental analysis and spectroscopic methods. The magnetite (Fe3O4) nanoparticles were prepared by the hydrothermal and solvothermal (in ionic liquid [BMIM][PF6]) methods from (BMIM)4[Fe(CN)6] as a precursor. The nanoparticles were characterized by X-ray diffraction (XRD), FT-IR, and scanning electron microscopy (SEM). The results show that the preparation of magnetite using the solvothermal method in [BMIM][PF6] has more advantages such as smaller size and high purity. https://jpst.irost.ir/article_80_f033ab37c30201f73f142449d037028d.pdf